Nano Crystal Characterization

3D precession electron diffraction tomography with ADT3D analysis

Ab-initio crystal structure determination

Enabling technique towards solving nanocrystal structures

Manual acquisition of tomographic data sets of (precession) electron diffraction patterns

Acquisition of diffraction patterns with quasi-kinematical (X-ray like) intensities

Analysis of tomographic data sets via ADT3D visualization and analysis software developed by Dr. Ute Kolb from Uni Mainz Germany

3D reciprocal space reconstruction
unit cell parameter determination
automatic measurements of the reflection intensities

Much smaller crystals can be analyzed with TEM versus X-Ray Tools (Single Crystal XRD / SC-XRD or synchrotron)

Intuitive workflow

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E. Mugnaioli et al Angew. Chemie Int Ed (2012) 51 7041-7045
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